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Analysis of the volatile components of five Turkish Rhododendron species by headspace solid-phase microextraction and GC-MS (HS-SPME-GC-MS)

机译:通过顶空固相微萃取和GC-MS(HS-SPME-GC-MS)分析五个土耳其杜鹃花种的挥发性成分

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摘要

Volatile constituents of various solvent extracts (n-hexane, CH2Cl2, H2O) of 15 different\udorgans (leaves, flowers, fruits) of five Rhododendron species (Ericaceae) growing in Turkey\udwere trapped with headspace solid-phase microextraction (HS-SPME) technique and analyzed\udby GC-MS. A total of 200 compounds were detected and identified from organic extracts,\udwhile the water extracts contained only traces of few volatiles. The CH2Cl2 extract of\udthe R. luteum flowers was found to exhibit the most diverse composition: 34 compounds\udwere identified, with benzyl alcohol (16.6%), limonene (14.6%) and p-cymene (8.4%) being\udthe major compounds. The CH2Cl2-solubles of R. x sochadzeae leaves contained only phenyl\udethyl alcohol. This study indicated appreciable intra-specific variations in volatile compositions\udwithin the genus. Different anatomical parts also showed altered volatile profiles. This\udis the first application of HS-SPME-GC-MS on the volatiles of Rhododendron species.
机译:用顶空固相微萃取(HS-SPME)捕获了土耳其生长的五种杜鹃花科的15种不同\ udorgans(叶子,花朵,水果)的各种溶剂提取物(正己烷,CH2Cl2,H2O)的挥发性成分)技术并通过GC-MS分析\ udp。从有机提取物中共检测和鉴定了200种化合物,\而水提取物中仅含有微量的挥发物。发现黄麻花的CH2Cl2提取物表现出最多样化的组成:鉴定出34种化合物,其中以苯甲醇(16.6%),柠檬烯(14.6%)和对伞花烯(8.4%)为主要化合物。虎杖叶的CH 2 Cl 2可溶物仅包含苯基\二乙醇。该研究表明该属中挥发性成分的明显种内变异。不同的解剖部位也显示出挥发性的变化。这是HS-SPME-GC-MS在杜鹃花种挥发物上的首次应用。

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